Experiment 8 : Ramen spectrographic analysis Objective: To utilize Raman Spectroscopy as an analytic chemistry tool to determine (i) the writing of an uncharted put out/ benzol mixture (ii) the amount of ethyl alcohol in vodka. Pre-lab questions: 1) What is a calibration curve and how would you go close to constructing iodin? A calibration curve shows the response of an analytical system to known quantities of an analyte. To construct a calibration curve, we beginning grind away known samples of the analyte covering a stray of densitys expected for the unknowns and time the response of the analytical procedures of these standards to generate direct data. After the measurement is done, a linear graph of the signal data against analyte concentration is plotted. The concentration of the unknown sample is then(prenominal) determined exploitation the equation of the calibration curve. Data assembling: (i) immersion of benzene (% volume) 5 10 20 30 40 60 70 80 Benzene /chloroform mixture rule book of benzene added 0.5 mL 1 mL 2 mL 3 mL 4 mL 6 mL 7 mL 8 mL Wave number(cm1) 1586.712262 1586.712262 1586.712262 1586.712262 1586.712262 1586.712262 1586.712262 1586.712262 summit counts 62.9508 48.53701 107.7373 137.6723 183.4448 279.8358 360.6083 392.8723 Concentration Volume of of centiliter (% chloroform volume) added 95 90 80 70 60 40 30 20 9.

5 mL 9 mL 8 mL 7 mL 6 mL 4 mL 3 mL 2 mL Wave number(cm1) 760.5276014 760.5276014 760.5276014 760.5276014 760.5276014 760.5276014 760.5276014 760.5276014 Peak counts 854.4691 629.294 742.5334 655.9348 613.8774 440.0543 374.7844 270.9479 unfathomable benzene/chloroform sample wave number (cm-1) lift count s 1586.712262 293.2169 760.5276014 431.0592 ! (ii) Ethanol Concentration of ethanol (% volume) 10 15 20 30 40 50 60 70 80 Volume of ethanol added 1.0 mL 1.5 mL 2.0 mL 3.0 mL 4.0 mL 5.0 mL 6.0 mL 7.0 mL 8.0 mL Volume of irrigate added 9.0 mL 8.5 mL 8.0 mL 7.0 mL 6.0 mL 5.0 mL 4.0 mL 3.0 mL 2.0 mL Wave number(cm-1) 880.8988764 880.8988764 880.8988764 880.8988764...If you want to get a full essay, order it on our website:
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